| 1. Identity statement | |
| Reference Type | Journal Article |
| Site | plutao.sid.inpe.br |
| Holder Code | isadg {BR SPINPE} ibi 8JMKD3MGPCW/3DT298S |
| Identifier | J8LNKAN8RW/3D545LE |
| Repository | dpi.inpe.br/plutao/2012/11.28.19.14 (restricted access) |
| Last Update | 2013:02.15.11.51.02 (UTC) administrator |
| Metadata Repository | dpi.inpe.br/plutao/2012/11.28.19.14.01 |
| Metadata Last Update | 2018:06.05.00.02.13 (UTC) administrator |
| Secondary Key | INPE--PRE/ |
| DOI | 10.1016/j.colsurfa.2012.09.041 |
| ISSN | 0927-7757 |
| Label | lattes: 9039822138866007 1 ArantesAPLLPCLL:2012:SyOpCo |
| Citation Key | ArantesPinLeiLonCam:2012:SyOpCo |
| Title | Synthesis and optimization of colloidal silica nanoparticles and their functionalization with methacrylic acid  |
| Year | 2012 |
| Month | Dec. |
| Access Date | 2024, Apr. 26 |
| Secondary Type | PRE PI |
| Number of Files | 1 |
| Size | 1303 KiB |
| 2. Context | |
| Author | 1 Arantes, Tatiane Moraes 2 Pinto, Alexandre H. 3 Leite, Edson R. 4 Longo, Elson 5 Camargo, Emerson R. |
| Group | 1 CMS-ETES-SPG-INPE-MCTI-GOV-BR |
| Affiliation | 1 Instituto Nacional de Pesquisas Espaciais (INPE) / LIEC - Laboratório Interdisciplinar de Eletroquímica e Cerâmica, Department of Chemistry, UFSCar-Federal University of São Carlos 2 LIEC - Laboratório Interdisciplinar de Eletroquímica e Cerâmica, Department of Chemistry, UFSCar-Federal University of São Carlos, Rod. Washington Luis km 235, CP 676, São Carlos, SP 13565-905, Brazil 3 LIEC - Laboratório Interdisciplinar de Eletroquímica e Cerâmica, Department of Chemistry, UFSCar-Federal University of São Carlos, Rod. Washington Luis km 235, CP 676, São Carlos, SP 13565-905, Brazil 4 LIEC-IQ, Chemistry Institute of Araraquara, Department of Biochemistry and Technological Chemistry, UNESP - São Paulo State University 5 LIEC-IQ, Chemistry Institute of Araraquara, Department of Biochemistry and Technological Chemistry, UNESP - São Paulo State University, Rua Francisco Degni, CP 355, Araraquara, SP 14801-907, Brazil |
| Author e-Mail Address | 1 tatiane.arantes@las.inpe.br |
| e-Mail Address | tatiane.arantes@las.inpe.br |
| Journal | Colloids and Surfaces A, Physicochemical and Engineering Aspects |
| Volume | 415 |
| Number | 5 |
| Pages | 209-217 |
| Secondary Mark | B1_CIÊNCIAS_BIOLÓGICAS_I B2_CIÊNCIAS_BIOLÓGICAS_II A2_ENGENHARIAS_I A1_ENGENHARIAS_II B1_ENGENHARIAS_III B1_FARMÁCIA A2_GEOCIÊNCIAS A1_INTERDISCIPLINAR B1_MATERIAIS B1_MEDICINA_I B2_QUÍMICA |
| History (UTC) | 2012-11-28 23:06:35 :: lattes -> marciana :: 2012 2013-02-15 11:53:54 :: marciana -> administrator :: 2012 2018-06-05 00:02:13 :: administrator -> marciana :: 2012 |
| 3. Content and structure | |
| Is the master or a copy? | is the master |
| Content Stage | completed |
| Transferable | 1 |
| Content Type | External Contribution |
| Version Type | publisher |
| Keywords | silica nanoparticles factorial design particle size surface functionalization |
| Abstract | The synthesis of colloidal SiO2 nanoparticles was achieved via the base-catalyzed hydrolysis and polycondensation of tetraethyl orthosilicate (TEOS) in an alcoholic medium with the careful variation of the concentrations of water, ammonia and TEOS. In this study, we investigated the influence of experimental parameters on the average size of nanoparticles by means of a multivariate statistical analysis using a factorial design to create one model to predict particle size in function of experimental conditions. This model predicted that it is possible to synthesize silica nanoparticles with size in the range from 17 to 333 nm, according to the chosen condition for the amount of water, ammonia and TEOS. It was observed that only the molar amount of NH3, the molar amount of H2O and the effect from interaction between molar amount of TEOS and H2O were significant. Subsequently, surface modification of the colloidal silica was performed in situ using the coupling agent 3(trimethoxysilyl)propyl methacrylate (TMSPM). |
| Area | FISMAT |
| Arrangement | urlib.net > BDMCI > Fonds > Produção pgr ATUAIS > CMS > Synthesis and optimization... |
| doc Directory Content | access |
| source Directory Content | there are no files |
| agreement Directory Content | there are no files |
| 4. Conditions of access and use | |
| Language | en |
| User Group | administrator lattes marciana |
| Visibility | shown |
| Archiving Policy | denypublisher denyfinaldraft24 |
| Read Permission | deny from all and allow from 150.163 |
| Update Permission | not transferred |
| 5. Allied materials | |
| Next Higher Units | 8JMKD3MGPCW/3F358GL |
| Dissemination | PORTALCAPES |
| Host Collection | dpi.inpe.br/plutao@80/2008/08.19.15.01 |
| 6. Notes | |
| Empty Fields | alternatejournal archivist callnumber copyholder copyright creatorhistory descriptionlevel format isbn lineage mark mirrorrepository nextedition notes orcid parameterlist parentrepositories previousedition previouslowerunit progress project readergroup resumeid rightsholder schedulinginformation secondarydate session shorttitle sponsor subject targetfile tertiarymark tertiarytype typeofwork url |
| 7. Description control | |
| e-Mail (login) | marciana |
| update | |
