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1. Identity statement
Reference TypeJournal Article
Sitemtc-m16.sid.inpe.br
Holder Codeisadg {BR SPINPE} ibi 8JMKD3MGPCW/3DT298S
Identifier6qtX3pFwXQZ3r59YDa/Hb2tS
Repositorysid.inpe.br/iris@1916/2005/08.16.12.36   (restricted access)
Last Update2005:08.16.03.00.00 (UTC) administrator
Metadata Repositorysid.inpe.br/iris@1916/2005/08.16.12.36.52
Metadata Last Update2018:06.05.01.16.07 (UTC) administrator
Secondary KeyINPE-12966-PRE/8245
ISSN0254-0584
Citation KeySilvaZane:2005:BiZiNi
TitleBismuth zinc niobate pyrochlore Bi1.5ZnNb1.5O7 from a polymeric urea-containing precursor
ProjectSUCERA: Ciência e engenharia de superfícies de sólidos e de cerâmicas micro e nanoestruturadas / Cerâmicas nanoestruturadas
Year2005
MonthOct.
Access Date2024, Apr. 28
Secondary TypePRE PI
Number of Files1
Size258 KiB
2. Context
Author1 Silva, S. A.
2 Zanetti, Sonia Maria
Group1 LAS-INPE-MCT-BR
2 LAS-INPE-MCT-BR
Affiliation1 Instituto Tecnológico de Aeronáutica, Centro Técnico Aeroespacial (ITA.CTA)
2 Instituto Nacional de Pesquisas Espaciais, Laboratório Associado de Sensores e Materiais, (INPE.LAS)
JournalMaterials Chemistry and Physics
Volume93
Number93
Pages2005
History (UTC)2006-01-04 12:24:48 :: sergio -> administrator ::
2006-09-28 22:30:10 :: administrator -> sergio ::
2008-01-07 12:52:55 :: sergio -> marciana ::
2008-02-19 18:20:24 :: marciana -> administrator ::
2018-06-05 01:16:07 :: administrator -> marciana :: 2005
3. Content and structure
Is the master or a copy?is the master
Content Stagecompleted
Transferable1
Content TypeExternal Contribution
KeywordsMATERIALS PHYSICS
Bi2O3-ZnO-Nb2O5
Urea
Pyrochlore
Nanopowder
Polymeric precursor
FÍSICA DE MATERIAIS
Pirocloro
Precursos polimérico
AbstractCubic bismuth zinc niobate pyrochlore (Bi1.5ZnNb1.5O7) nanopowder was synthesized by a urea-modified polymeric precursor method. The pH of the chemical solution was stabilized through the homogeneous decomposition of urea, and the influence of the urea content was evaluated. The powders were obtained after pre-treatment at 300 and 400 degrees C for 4 h, followed by heat treatment at different temperatures (500, 600 and 700 degrees C) for 2 h. The DSC results indicate that the cubic pyrochlore phase (alpha-BZN) crystallizes at temperatures as low as 500 degrees C. The crystallization process was followed by XRD, which revealed that no detectable intermediary phases such as BiNbO4 or a pseudo-orthorhombic pyrochlore were observed at any time. The powder obtained presents large agglomerates of clusters of nanoparticles of around 50 nm, which were examined by TEM.
AreaFISMAT
Arrangementurlib.net > BDMCI > Fonds > Produção anterior à 2021 > LABAS > Bismuth zinc niobate...
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4. Conditions of access and use
Languageen
Target FileBismuth zinc niobate.pdf
User Groupadministrator
marciana
sergio
Visibilityshown
Copy HolderSID/SCD
Archiving Policydenypublisher denyfinaldraft24
Read Permissiondeny from all and allow from 150.163
5. Allied materials
Next Higher Units8JMKD3MGPCW/3ESR3H2
DisseminationWEBSCI
Host Collectionsid.inpe.br/banon/2003/08.15.17.40
6. Notes
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7. Description control
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