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1. Identity statement
Reference TypeJournal Article
Sitemtc-m16d.sid.inpe.br
Holder Codeisadg {BR SPINPE} ibi 8JMKD3MGPCW/3DT298S
Identifier8JMKD3MGP7W/3A7GMKL
Repositorysid.inpe.br/mtc-m19/2011/08.03.17.54   (restricted access)
Last Update2011:10.19.10.15.50 (UTC) administrator
Metadata Repositorysid.inpe.br/mtc-m19/2011/08.03.17.54.56
Metadata Last Update2021:02.10.18.35.30 (UTC) administrator
Secondary KeyINPE--PRE/
DOI10.1016/j.apsusc.2011.04.090
ISSN0169-4332
Citation KeyAntunesReMeCuCoMa:2011:AnReIr
TitleAnalyses of residual iron in carbon nanotubes produced by camphor/ferrocene pyrolysis and purified by high temperature annealing
Year2011
MonthJuly
Access Date2024, May 05
Secondary TypePRE PI
Number of Files1
Size1363 KiB
2. Context
Author1 Antunes, E. F.
2 Resende, V. G.
3 Mengui, U. A.
4 Cunha, J. B. M.
5 Corat, E. J.
6 Massi, M.
Group1 LAS-CTE-INPE-MCT-BR
2 CPT-CPT-INPE-MCT-BR
3 LAS-CTE-INPE-MCT-BR
4
5 LAS-CTE-INPE-MCT-BR
6 LAS-CTE-INPE-MCT-BR
Affiliation1 Instituto Nacional de Pesquisas Espaciais (INPE)
2 Instituto Nacional de Pesquisas Espaciais (INPE)
3 Instituto Nacional de Pesquisas Espaciais (INPE)
4
5 Instituto Nacional de Pesquisas Espaciais (INPE)
6 Instituto Nacional de Pesquisas Espaciais (INPE)
Author e-Mail Address1
2
3
4 Univ Fed Rio Grande do Sul, BR-91501970 Porto Alegre, RS, Brazil
e-Mail Addresssecretaria.cpa@dir.inpe.br
JournalApplied Surface Science
Volume257
Number18
Pages8038-8043
History (UTC)2011-11-03 13:33:10 :: secretaria.cpa@dir.inpe.br -> administrator :: 2011
2021-02-10 18:35:30 :: administrator -> marciana :: 2011
3. Content and structure
Is the master or a copy?is the master
Content Stagecompleted
Transferable1
Content TypeExternal Contribution
Version Typepublisher
KeywordsRAMAN-SPECTRA
MOSSBAUER-SPECTROSCOPY
PURIFICATION
PRESSURE
CARBIDES
PLASMA
GROWTH
BAND. Carbon nanotubes
Purification
Annealing
Mossbauer spectrocopy
Camphor
XPS
AbstractA detailed analysis of iron-containing phases in multiwall carbon nanotube(MWCNT) powder was carried out. The MWCNTs were produced by camphor/ferrocene and purified by high temperature annealing in an oxygen-free atmosphere (N(2) or VC). Thermogravimetric analysis, Mossbauer spectroscopy, X-ray diffraction and X-ray photoelectron spectroscopy enabled the evaluation of the residual iron in MWCNTs after purification. The VC treatments provided MWCNTs with a purity degree higher than 99%. Moreover, Raman spectroscopy revealed a significant improvement in graphitic ordering after thermal annealing. A brief description of the mechanism of iron removal was included. We highlight the mobility of iron atoms through graphitic sheets and the large contact angle of iron clusters formed on MWCNT surfaces at high temperatures. (C) 2011 Elsevier B.V. All rights reserved.
AreaFISMAT
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Languageen
User Groupadministrator
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5. Allied materials
Mirror Repositorysid.inpe.br/mtc-m19@80/2009/08.21.17.02.53
Next Higher Units8JMKD3MGPCW/3ESR3H2
8JMKD3MGPCW/3EUPEJL
DisseminationWEBSCI; PORTALCAPES; COMPENDEX.
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6. Notes
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